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Now we can freely grow any herb for our own use and enjoyment as our Creator intended For in the process of understanding TRUTH is revealed ure to cool,
then pour it into a sep funnel. Wash the ethyl acetate solution with 50
ml of water to recover the lithium iodide into the water solution.
Separate off the water layer, and evaporate the water to recover the
lithium iodide for reuse. The ethyl acetate solution should be dried
over some anhydrous sodium sulfate, then the ethyl acetate evaporated
off to give about 20 grams of 2,4,5-trimethoxyphenlyacetone. This
light-sensitive substance should be stored in the freezer.
12 Studies On The Production OfTMA-2
Acetonitrile is a quite poisonous solvent, dangerous both in
inhalation from the fizzing electrochemical cell and by absorption
through the skin. It has been my experience that just spilling a little bit of
it on your skin is enough to give you head rushes and make you feel
uncomfortable. The use of acetonitrile can be avoided without loss of
yield by using the alternative procedure in Example 6 in the patent.
The electrochemical cell is constructed in exactly the same way as in
the first method. Then into the electrochemical cell put 400 ml of
dimethylformamide, 200 ml of water containing 27 grams NaBr, and 20
grams asarone. Check the level of the solution, and make sure that the
amount of electrode surfaces are the same as in the first method. Then
begin stirring, and pass the current through the solution exactly as in the
When the 24,000 coulombs have been passed, pour the contents of
the beaker into a sep funnel, dilute with 1000 ml of a 20% solution of
salt in water, and extract four times with 200 ml portions of ethyl
acetate. The combined extracts, amounting to 800 ml, should be
washed twice with 200 ml portions of a 20% solution of salt in water.
The ethyl acetate solution contains the product epoxide. It should be
evaporated under a vacuum to a volume of about 200 ml, then reacted
with lithium iodide just as in the first method to yield about 20 grams of
Recycling of solvents is possible with this method too. Ethyl
acetate can be recovered during the vacuum evaporation by use of a
dry-ice trap. The dimethyl-formamide can be recovered by vacuum
The Journal Method
A very effective alternative method exists for converting propenyl
benzenes to phenylacetones. I know through mail received from the
reading public that this method gives a yield of about 80% when used
Practical LSD Manufacture
with isosafrole. Similar results can be expected when used with
In spite of the high yields and simplicity of this reaction, I can't
recommend its use. That's because this procedure uses thallium(III)
nitrate to oxidize the propenylbenzene to the corresponding
phenylacetone. The thallium(III) nitrate gets reduced to thallium(I)
nitrate. Both of these heavy-metal compounds are very poisonous and,
unlike organic chemicals, the heavy metals persist forever in the
environment, and accumulate in the body. You wa