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LSD From Lysergic Acid And
This method also appears to work via some kind of mixed
anhydride. The authors of the US patent 3,141, 887 from which this is
taken didn't investigate the nature of the intermediate formed between
anhydrous lysergic acid and phosgene, but the similarities between
this method and those using SOs
or trifluoroacetic anhydride are
obvious. As in those methods, lysergic acid reacts with about two
molecules of phosgene to form an intermediate which is then reacted
with diethylamine to yield LSD. According to the patent, it is not
crucial for success to use the exact stoichiometric amount of phosgene in
reaction with lysergic acid. A ratio of about 2-1 phosgene to
lysergic acid gives best results, but anything fairly close to that works
just fine too.
This is not a method to get excited about.
Phosgene is a very
sneaky poison which is best suited to assassination or wholesale
chemical assault, not the home synthesis of drugs. Phosgene is not
irritating when inhaled, and has delayed effects which easily lead to
For a complete treatment of the poisonous properties of
phosgene, read Silent Death by me. This substance should not be used
without very effective ventilation. Smoking while in its presence
serves as a warning device, as phosgene makes the smoke taste bad.
One can also prepare a
warning paper by soaking said paper in an
Practical LSD Manufacture
alcohol solution containing 10% of an equal mixture of p-dimethylaminobenzaldehyde
and colorless diphenylamine. This paper is then
dried. It will turn yellow to deep orange in the presence of the
maximum-allowable concentration of phosgene.
It is a good idea to
wear this paper while working. The only justification of choosing this
method is if a cylinder of phosgene gas is very easily available at work or
To do this reaction, a carefully dried 500 ml flask is charged with a
magnetic stirring bar, 5 grams of anhydrous lysergic acid dried
under heat and high vacuum as described in the previous chapter, and
100 ml dimethlyformamide.
Stopper the flask, and cool it to -10° C in a
salt-ice bath. The lysergic acid will not dissolve.
Next to this flask attach a dropping funnel, and drip in 20 ml of
dimethylformamide containing 3.4 grams of phosgene. This solution is
best prepared by taking 200 ml of dimethylformamide and slowly
bubbling into it Premiumbalikratomsoldindestin
dimethylformamide phosgene from a cylinder until
the solution gains 34 grams weight. Strong stirring during the
bubbling helps to ensure that most of the phosgene goes into solution
and not the surrounding air. The exact concentration of this phosgene-
DMF complex is unimportant; what is important is that the weight
gain be known, and the amount then portioned out into the batch
contain 3.4 grams phosgene. The addition of the phosgene complex
into the lysergic acid suspension should take at least 20 minutes.
The addition of phosgene should bring
Our original mission to promote Legal High herbs as safe alternatives to harmful illegal and legal drugs escalated to a cause when we suddenly became aware of the oppression and restrictions forced onto natural herb and remedies by the political lobbying and biased influence from powerful and sinister profit driven pharmaceutical corporations