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and let the rice cakes slowly shift through the
fruiting temperature range. Note that everything else must be right.
The rice cake must have a fully developed mycelium network and
there must be light. The Ice-Pak should be placed between 1/4 and 1/2
inch from the rice cakes. A flat Ice-Pak will work, but if you have the
option, get one that is designed to slip into the center of a six-pak. It
will have circular indents molded into each side and it will conform to
the shape of the rice cakes better. If everything was ready, you should
see pin heads develop 3 or 4 days after you perform this adaptation. If
you don't see any develop after 3 or 4 days, you can repeat this
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How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
operation again. The networks may not have been developed full
enough and the few days since the last attempt may have been enough
time to change this fact.
Advantage:
You can still initiate prolific flushes with the terrarium above the
normal temperature range. The optimum temperature for growing
mushrooms is higher than what is necessary to initiate new
mushrooms and is between 80 and 90 degrees F. This adaptation can
let the cultivator grow at the maximum rate, and still produce new
mushrooms on the cakes.
Disadvantages:
The Ice-Pak will lower the humidity in the terrarium. Mostly, this is
an issue when you have mushrooms on cakes that are part way
through the growing cycle and not ready to harvest. They will usually
survive the bad growing conditions for the six hours it takes the Ice-
Pak to initiate fruiting, but they will suffer for it. You need to have an
ultra sonic humidifier setup on your terrarium. Nothing else will be
able to keep the humidity high enough. You can turn the humidity
control up a little, but you will have to continue to adjust it down as
the Ice-Pak loses its cool. If too much moisture forms on the cakes, it
will prevent the initiation of pin heads and that was the whole purpose
of this operation.
Back to the Growing Cycle.
table of contents.
Adaptation-17: Adding Moisture to the Rice Cake.
After a cake has produced several mushrooms you can add moisture
to it. Flame sterilize a 3/16 inch drill bit. Let it cool. Use it to drill a
hole at the center of the cake. You can do this by hand. You do not
need a drill. Do not go all the way through the cake, but drill a deep
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How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
reservoir into the cake. Cut a plastic straw to 4 inches in length. Insert
the straw 1/2 inch into the hole. The straw should fit tightly in the
cake. Straws from McDonalds are larger than most and work well.
They seal well and hold more water. Fill the straw with water daily. A
10 cc. syringe works well to fill the straws with water. You should
wait to drill the hole until the cake has produced some mushrooms
because the inside of the rice See
the following diagram:
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How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 2)
That is it. The basic grow chamber is done. Now you need to decide
which method you are going to use to keep the humidity high and the
CO2 concentration low while the mushrooms are growing.
Method 1: Hand Spraying.
This is the original method that Psylocybe Fanaticus recommended for
the home cultivator to grow mushrooms. It is the least expensive. It is
the most labor intensive and forces you to conform to a demanding
schedule. The only thing you need in addition to the basic growing
chamber is a spray bottle that can put out a fine mist.
The procedure is this: At least four times a day the terrarium needs to
have humidity injected into it via the spray bottle. At least twice a day
the CO2 that has built up needs to be eliminated. Once a day you need
to eliminate water from the bottom of the terrarium that has condensed
and formed there.
Once a day, you need to remove the standing water from the bottom of
the terrarium. You can use a turkey baster to suck the water out, or you
can gently remove each cake and turn the terrarium up side down to
drain the water out. If you remove the cakes, be very gentle. Any place
you touch the cakes will not fruit. You should pick up the cakes in the
same place every time.
Twice a day, the CO2 that has accumulated in the chamber needs to be
removed. One method is to remove the drip shield and fan the inside of
the cooler with the cover for 10 or 15 seconds. Another method that
works well is to have a hair dryer next to the cooler and use it. Simply
lower it into the terrarium with the exhaust jet pointing up and out of
the terrarium and turn it on. It will suck all the existing CO2 out of the
chamber. Be sure not to hit the rice cakes with the hot exhaust air. It
(15 of 29) 5/1/2002 6:54:17 PM
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 2)
will damage them. If your hair dryer has a 'cool' setting, use that
instead of 'hot'. Incidentally, one cultivator recommends using a
vacuum clean instead. He would simply suck the stale air out of the
terrarium.
In order to create humidity in the terrarium a spray bottle that is
capable of generating a fine mist is used. There are a lot of different
products for use in the kitchen that have an adjustable spray nozzle,
but if you choose to recycle one of these, make sure it produces a very
fine mist. What ever you use, make sure it is entirely clean of the
original chemicals. Let's make this perfectly clear. Make sure the bottle
is clean and does not contain anything that will damage the fungus.
The safest thing to do is go to the hardware store and buy a high
quality spray bottle. These typically produce a finer mist than most
kitchen type spray bottles. The problem is that you would not be using
a spray bottle if you had a little extra cash so we are telling you that
you ca
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ically. Add 500 ml of hexane to the flask, and distill
off about half of it, using a fractionating column. Both water and
methanol form azeotropes with hexane.
The approximately 250 mis of solution left in the flask is now
cooled in an ice bath to about 5° C. When that temperature is reached, . 1
mole of SOa-acetonitrile complex is added. If the solution prepared is .5-
molar strength, that requires the addition of 200 ml. This
addition should be done with strong magnetic stirring, and slowly
enough that the temperature does not climb too much. After the SOa
has been added, allow the reaction to come to completion for about 5
minutes, then add 18 grams of diethylamine (26 ml) dissolved in 250
ml of anhydrous ether.
A further 5 minutes of reaction time is then allowed with stirring,
before pouring the whole reaction mixture into a 2000 ml sep funnel.
Now 1000 ml of water is slowly poured into the sep funnel with
swirling. This addition of water generates a lot of heat as the SOs
reacts to make sulfuric acid, and then gets diluted. Over a period of
time work up to shaking the sep funnel. The LSD goes into the water
layer. Separate it off, and extract four more times with 1000 ml
portions of water.
The combined water extracts (5000 ml in all) are now saturated
with salt, then extracted five times with 1000 ml portions of ethylene
dichloride (1,2-dichloro-ethane). Ethylene dichloride is heavier than
water, so it forms the lower layer in the sep funnel.
Practical LSD Manufacture
54
The ethylene dichloride now contains the LSD. Check the
extracted solutions with a blacklight to make sure they have been
completely extracted. This solvent is now removed under vacuum (a
rotovap makes this much easier, but is not the sort of thing one gets at a
garage sale). Warm water can be used to heat the flask during the
vacuum evaporation.
The residue in the flask is a mixture of LSD and iso-LSD. The
isomeric mixture comes from using isomerically-mixed lysergic acid.
The iso-LSD is separated from the LSD using the chromatographic
method given in Chapter 4, and the iso-LSD converted to LSD by the
method also given in that chapter. Conversion to the tartarate salt is
also done in the same way as described in Chapter 4.
Journal Method
In this method, the formation of the metal salt of lysergic acid is
done exactly as given above. Now to the residue left in the flask after
vacuum evaporation of the methanol, add 500 ml of
dimethylformamide. Half of the dimethylformamide is now distilled
off under a vacuum through a fractionating column to remove traces of
water and methanol. Aspirator vacuum is strong enough for this
distillation, but beware of the tendency for formamides to bump
during vacuum distillations. The vacuum should be strong enough
that the dimethylformamide distills at around 50° C.
Now cool the formamide solution, and when it has cooled to 5° C,
add 100 ml of 1M SCvformamide complex. Allow 10 minutes of
stirr
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