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the Wherecanibuybathsaltnoveltypowderforinlosangelesca top of the drum are two threaded openings. Opening number one is
secured with the original bung. The other opening is tightly stuffed with
a rubber stopper. This rubber stopper has a hole drilled in it, and a
section of pipe is put through the hole in the stopper so that it
Extraction And Isolation Of
The Lysergic Acid Amides
extends about an inch below the stopper. To this pipe, a line of
vacuum tubing is attached, leading to a vacuum pump. This pump
should be the typical shop pump that can pull a vacuum of about 21
inches of mercury out of the possible 30 inches.
This is enough to
greatly speed the evaporation without causing the chloroform to boil.
Boiling may raise a head of foam that would carry product along with it,
causing great losses.
On a laboratory scale, a stronger vacuum can be used from an
aspirator. By using red or yellow darkroom light bulbs for
illumination, damage to the product can be kept to a minimum. The
stronger vacuum speeds up the process quite a bit. Use boiling chips to
As the chloroform evaporates away, more of the extraction solvent
may be added to either the 55-gallon drum or the distilling flask,
depending upon the scale of production.
The evaporation is continued
until the extraction solvent has been reduced to one-fifteenth its
For the 200-pound crop, the 150 gallons of extraction
solvent has been reduced to 10 gallons.
An accessory which may speed up and smooth out this
evaporation is a capillary air bubbler. This is made by taking a section of
glass tubing, and poking it through a rubber stopper.
The end of the
glass tubing is then heated to redness in a flame, and pulled into a
very fine capillary. The tubing is then stuck into the solution being
evaporated, extending nearly to the bottom.
The vacuum will pull a
fine stream of air bubbles through the solution and aid evaporation.
When the chloroform has been reduced to one-fifteenth of its
original volume, it must be diluted Wheretobuycrystaalbubbly with ether. The reason for this is
that the next step is extraction of the ergot alkaloids into a tartaric-acid
solution, and it has been found that this is very difficult from pure
chloroform. When the solution is predominantly ether, the transfer of
the alkaloids into the tartaric-acid solution can be done efficiently. For
the drum-sized batch, add 30 gallons of ether and two gallons of
alcohol. Similarly, for smaller batches add three volumes of ether and a
At this point, an important matter must be addressed. This matter is
central snoopervision of chemical transactions. Note the "Love
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Letters From The Heat" section at the end of this book concerning the
Chemical Diversion Trafficking Act of 1988, and its amendments
since then. This federal law requires chemical dealers to "identify
their customers, maintain retrievable records, and report suspicious
transactions" for a list of chemicals compiled a